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(R)-N-BOC-2-methylproline

Base Information Edit
  • Chemical Name:(R)-N-BOC-2-methylproline
  • CAS No.:166170-15-6
  • Molecular Formula:C11H19NO4
  • Molecular Weight:229.276
  • Hs Code.:
  • Mol file:166170-15-6.mol
(R)-N-BOC-2-methylproline

Synonyms:1,2-Pyrrolidinedicarboxylicacid, 2-methyl-, 1-(1,1-dimethylethyl) ester, (R)-;(R)-Boc-2-methylproline;

Suppliers and Price of (R)-N-BOC-2-methylproline
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • (R)-1-(tert-Butoxycarbonyl)-2-methylpyrrolidine-2-carboxylicAcid
  • 50mg
  • $ 60.00
  • SynQuest Laboratories
  • 1-Boc-2-methyl-D-proline
  • 250 mg
  • $ 175.00
  • SynQuest Laboratories
  • 1-Boc-2-methyl-D-proline
  • 1 g
  • $ 575.00
  • Matrix Scientific
  • 1-Boc-2-methyl-D-proline
  • 1g
  • $ 662.00
  • Crysdot
  • (R)-1-(tert-Butoxycarbonyl)-2-methylpyrrolidine-2-carboxylicacid 97%
  • 25g
  • $ 218.00
  • Crysdot
  • (R)-1-(tert-Butoxycarbonyl)-2-methylpyrrolidine-2-carboxylicacid 97%
  • 100g
  • $ 713.00
  • ChemPep
  • Boc-α-Me-D-Pro-OH
  • 1g
  • $ 726.00
  • ChemPep
  • Boc-α-Me-D-Pro-OH
  • 5g
  • $ 1778.00
  • Biosynth Carbosynth
  • Boc-a-Me-D-Pro-OH
  • 2 g
  • $ 160.00
  • Biosynth Carbosynth
  • Boc-a-Me-D-Pro-OH
  • 1 g
  • $ 95.00
Total 53 raw suppliers
Chemical Property of (R)-N-BOC-2-methylproline Edit
Chemical Property:
  • Melting Point:127-129℃ 
  • Boiling Point:337.762 °C at 760 mmHg 
  • PKA:4.20±0.20(Predicted) 
  • Flash Point:158.073 °C 
  • PSA:66.84000 
  • Density:1.16g/cm3 
  • LogP:1.79850 
  • Storage Temp.:2-8°C 
Purity/Quality:

99.9% *data from raw suppliers

(R)-1-(tert-Butoxycarbonyl)-2-methylpyrrolidine-2-carboxylicAcid *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of (R)-N-BOC-2-methylproline

There total 5 articles about (R)-N-BOC-2-methylproline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 5%-palladium/activated carbon; hydrogen; In ethanol; at 20 ℃; under 2828.7 Torr; Inert atmosphere;
DOI:10.1021/acs.joc.8b02866
Guidance literature:
With tetramethyl ammoniumhydroxide; In acetonitrile; at 20 - 40 ℃;
Guidance literature:
Multi-step reaction with 3 steps
1.1: tert-butyl methyl ether / 25 °C
1.2: 1 h / 25 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0 °C
3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 20 °C / 2828.7 Torr / Inert atmosphere
With 5%-palladium/activated carbon; hydrogen; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; tert-butyl methyl ether;
DOI:10.1021/acs.joc.8b02866
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