3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

Base Information

Chemical Name:3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde
CAS No.:1268257-46-0
Molecular Formula:C₂₀H₂₈FN₃O₇
Molecular Weight:441.457
Hs Code.:

Synonyms:3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

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Chemical Property of 3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

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Technology Process of 3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

There total 2 articles about 3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1233816-91-5
1-azido-2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}-ethane

: 1268257-59-5
3,4-dimethoxy-5-prop-2-ynyloxy-benzaldehyde

: 1268257-46-0
3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium ascorbate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm101110w

Reference yield:

: 29865-90-5
3-hydroxy-4,5-dimethoxybenzaldehyde

: 1268257-46-0
3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

2: copper(ll) sulfate pentahydrate; sodium ascorbate / N,N-dimethyl-formamide / 20 °C

With copper(ll) sulfate pentahydrate; sodium ascorbate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm101110w

Reference yield: 27.0%

: 1268257-46-0
3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde

: 162256-49-7
2-benzo<1,3>dioxol-5-yl-4-(4-methoxyphenyl)-4-oxobutyric acid methyl ester

: 1268257-50-6
3-benzo[1,3]dioxol-5-yl-4-{-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-1,2,3-triazol-4-ylmethoxy]-4,5-dimethoxybenzyl}-5-hydroxy-5-(4-methoxyphenyl)-5H-furan-2-one

Guidance literature:: 3-[1-(2-{2-[2-(2-fluoroethoxy)ethoxy]ethoxy}ethyl)-1H-[1,2,3]triazol-4-ylmethoxy]-4,5-dimethoxybenzaldehyde; 2-benzo<1,3>dioxol-5-yl-4-(4-methoxyphenyl)-4-oxobutyric acid methyl ester; With sodium; In methanol; for 19h; Reflux;

With acetic acid; for 7h; Reflux;
DOI:10.1021/jm101110w