2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Base Information

Chemical Name:2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide
CAS No.:1027245-94-8
Molecular Formula:C₁₇H₂₃NO₄S
Molecular Weight:337.44
Hs Code.:

2,2-dimethyl-1a,7b-dihydro-2<i>H</i>-1,3-dioxa-cyclopropa[<i>a</i>]naphthalene-6-sulfonic acid cyclohexylamide

Synonyms:2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Suppliers and Price of 2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

There total 3 articles about 2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1025830-47-0
2,2-dimethyl-2H-chromene-6-sulfonic acid cyclohexylamide

: 1027245-94-8
2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Guidance literature:: With sodium hypochlorite; 4-Phenylpyridine 1-oxide; Jacobsen's catalyst; In water; at 0 ℃; for 18h; pH=11.3;
DOI:10.1021/jm990196h

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 1027245-94-8
2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 2 h / 20 °C

2: sodium hypochlorite; (S,S)-(+)-Jacobsen's catalyst; 4-phenylpyridine-N-oxide / H₂O / 18 h / 0 °C / pH 11.3

With sodium hypochlorite; 4-Phenylpyridine 1-oxide; Jacobsen's catalyst; In dichloromethane; water; 1: Acylation / 2: Epoxidation;
DOI:10.1021/jm990196h

Reference yield:

: 185316-64-7
2,2-dimethyl-2H-1-benzopyran-6-sulfonyl chloride

: 1027245-94-8
2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-sulfonic acid cyclohexylamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 2 h / 20 °C

2: sodium hypochlorite; (S,S)-(+)-Jacobsen's catalyst; 4-phenylpyridine-N-oxide / H₂O / 18 h / 0 °C / pH 11.3

With sodium hypochlorite; 4-Phenylpyridine 1-oxide; Jacobsen's catalyst; In dichloromethane; water; 1: Acylation / 2: Epoxidation;
DOI:10.1021/jm990196h