{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Base Information

Chemical Name:{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester
CAS No.:916516-00-2
Molecular Formula:C₄₃H₄₇Cl₃N₂O₆
Molecular Weight:794.215
Hs Code.:

Synonyms:{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Suppliers and Price of {2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of {2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

There total 4 articles about {2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: N-((tris(4-chlorophenyl)propionyl)glycyl)glycine

: 124389-14-6
4-[(11-hydroxyundecyl)oxy]benzaldehyde

: 916516-00-2
{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetone; at 20 ℃; for 24h;
DOI:10.1021/ol062284j

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 916516-00-2
{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃; NaI / dimethylformamide / 12 h / 100 °C

2: 66 percent / EDCI; DMAP / acetone / 24 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol062284j

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 916516-00-2
{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetic acid 11-(4-formyl-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃; NaI / dimethylformamide / 12 h / 100 °C

2: 66 percent / EDCI; DMAP / acetone / 24 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol062284j