tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

Base Information

Chemical Name:tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane
CAS No.:113237-54-0
Molecular Formula:C₆₀H₆₄P₄*4Cl
Molecular Weight:1050.88
Hs Code.:

Synonyms:tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

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Technology Process of tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

There total 2 articles about tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 113237-53-9
tetrachlorure d'octaphenyl-1,1,6,6,9,9,14,14 tetraphosphonia-1,6,9,14 cyclohexadecadiene-3,11

: 113237-54-0
tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

Guidance literature:: With hydrogen; nickel; at 20 ℃; for 2.5h; under 41253.3 Torr;
DOI:10.1016/S0040-4039(00)95340-1

Reference yield:

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 113237-54-0
tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / toluene / 4 h / Heating

2: 95 percent / Hydrogen / Raney-Ni / 2.5 h / 20 °C / 41253.3 Torr

With hydrogen; nickel; In toluene;
DOI:10.1016/S0040-4039(00)95340-1

Reference yield:

: 113237-54-0
tetrachlorure d'octaphenyl-1,1,4,4,9,9,12,12 tetraphosphonia-1,4,9,12 cyclohexadecane

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 4151-27-3
1,4-bis(diphenylphosphinyl)butane

Guidance literature:: With sodium hydroxide; In ethanol; for 14h; Yield given. Yields of byproduct given; Heating;
DOI:10.1016/S0040-4039(00)95340-1