3-Chloro-2-iodobenzoic acid

Base Information

Chemical Name:3-Chloro-2-iodobenzoic acid
CAS No.:123278-03-5
Molecular Formula:C7H4ClIO2
Molecular Weight:282.465
Hs Code.:2916399090
DSSTox Substance ID:DTXSID40560936
Nikkaji Number:J1.880.332A
Wikidata:Q82444587
Mol file:123278-03-5.mol

Synonyms:3-chloro-2-iodobenzoic acid;123278-03-5;3-CHLORO-2-IODO-BENZOIC ACID;BENZOIC ACID, 3-CHLORO-2-IODO-;MFCD06808824;3-Chloro-2-iodobenzoicacid;SCHEMBL1222476;DTXSID40560936;IHSNWQTZBUIFSL-UHFFFAOYSA-N;BCP20542;AKOS015909206;AB30453;DS-17033;SY102784;CS-0041180;A805039

Suppliers and Price of 3-Chloro-2-iodobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Chloro-2-iodobenzoicAcid
100mg
$ 110.00

SynQuest Laboratories
3-Chloro-2-iodobenzoic acid 98%
250 mg
$ 117.00

Labseeker
3-chloro-2-iodobenzoicacid 97
5g
$ 339.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
500mg
$ 149.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
250mg
$ 125.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
1g
$ 198.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
100mg
$ 98.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
50mg
$ 88.00

J&W Pharmlab
3-Chloro-2-iodo-benzoicacid 96%
5g
$ 798.00

Crysdot
3-Chloro-2-iodobenzoicacid 98%
5g
$ 665.00

Total 24 raw suppliers

Chemical Property of 3-Chloro-2-iodobenzoic acid

Chemical Property:

Boiling Point:360.5 °C at 760 mmHg
Flash Point:171.8 °C
PSA：37.30000
Density:2.077 g/cm³
LogP:2.64280
Storage Temp.:2-8°C(protect from light)
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:281.89445
Heavy Atom Count:11
Complexity:163

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-2-iodobenzoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)I)C(=O)O

Technology Process of 3-Chloro-2-iodobenzoic acid

There total 6 articles about 3-Chloro-2-iodobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 535-80-8
3-chlorobenzoate

: 13421-00-6
5-chloro-2-iodo-benzoic acid

: 123278-03-5
3-chloro-2-iodo-benzoic acid

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; iodine; silver(I) acetate; triethylamine; at 23 ℃; for 18h; regioselective reaction; Sealed tube;
DOI:10.1002/chem.202002204

Reference yield: 55.0%

: 535-80-8
3-chlorobenzoate

: 123278-03-5
3-chloro-2-iodo-benzoic acid

Guidance literature:: 3-chlorobenzoate; With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran; at -50 ℃; for 4h;

With iodine; In tetrahydrofuran; at -50 - 20 ℃; Further stages.;
DOI:10.1021/jo026514t

Reference yield:

: 6388-47-2
2-amino-3-chlorobenzoic acid

: 123278-03-5
3-chloro-2-iodo-benzoic acid

Guidance literature:: 2-amino-3-chlorobenzoic acid; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; for 0.5h; Inert atmosphere;

With sulfuric acid; potassium iodide; In water; at 10 - 90 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3ra42474j