2-iodo-3-nitro-benzoic acid

Base Information

• Chemical Name: 2-iodo-3-nitro-benzoic acid
• CAS No.: 5398-69-6
• Molecular Formula: C7H4 I N O4
• Molecular Weight: 293.018
• Hs Code.: 2916399090
• Mol file: 5398-69-6.mol

Synonyms:2-Iodo-3-nitrobenzoicacid; NSC 4539

Chemical Property of 2-iodo-3-nitro-benzoic acid

Chemical Property:

• Vapor Pressure: 1.23E-06mmHg at 25°C
• Melting Point: 207-212°C
• Boiling Point: 385.6°Cat760mmHg
• Flash Point: 187°C
• Density: 2.156g/cm³
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

95% ^*data from raw suppliers

2-Iodo-3-nitrobenzoic acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

Useful:

Technology Process of 2-iodo-3-nitro-benzoic acid

There total 11 articles about 2-iodo-3-nitro-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Iodobenzoic acid (88-67-5) → 2-iodo-5-nitro-benzoic acid (19230-50-3) + 2-iodo-3-nitrobenzoic acid (5398-69-6)

Guidance literature:

With sulfuric acid; nitric acid; at 135 ℃; for 1h;

DOI:10.1039/c2dt32422a

Reference yield:

C7H5N2O4(1-)*K(1+) → 2-iodo-3-nitrobenzoic acid (5398-69-6)

Guidance literature:

C₇H₅N₂O₄^(1-)*K⁽¹⁺⁾; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 1.5h;

With iodine; potassium iodide; In water; dimethyl sulfoxide; at 5 - 50 ℃; for 0.666667h;

Reference yield:

→ 2-iodo-3-nitrobenzoic acid (5398-69-6)

Guidance literature:

With iodine; potassium iodide;

upstream raw materials:

3-nitroanthranilic acid

2-acetylamino-3-nitro-benzoic acid methyl ester

2-Iodobenzoic acid

3-nitrophthalic acid

Downstream raw materials:

methyl 2-iodo-3-nitrobenzoate

2-iodo-3-nitrobenzoyl chloride

(2-iodo-3-nitrophenyl)methanol

2-Benzylthio-3-nitrobenzoesaeure