4'-Bromo-4-iodobenzophenone

Base Information

• Chemical Name: 4'-Bromo-4-iodobenzophenone
• CAS No.: 609820-28-2
• Molecular Formula: C₁₃H₈BrIO
• Molecular Weight: 387.014
• DSSTox Substance ID: DTXSID10400294
• Nikkaji Number: J3.108.269B
• Wikidata: Q82203190
• Mol file: 609820-28-2.mol

Synonyms:4'-BROMO-4-IODOBENZOPHENONE;609820-28-2;(4-bromophenyl)-(4-iodophenyl)methanone;MFCD00510441;4-Iodo-4'-bromobenzophenone;SCHEMBL8143209;DTXSID10400294;AKOS009338674

Chemical Property of 4'-Bromo-4-iodobenzophenone

Chemical Property:

• Vapor Pressure: 4.56E-07mmHg at 25°C
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 385.88033
• Heavy Atom Count: 16
• Complexity: 240

Purity/Quality:

97% ^*data from raw suppliers

4'-Bromo-4-iodobenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)C2=CC=C(C=C2)I)Br

Technology Process of 4'-Bromo-4-iodobenzophenone

There total 1 articles about 4'-Bromo-4-iodobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(4-bromophenyl)-(4-iodophenyl)methanol (172483-73-7) → 4-bromo-4'-iodobenzophenone (609820-28-2)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;

DOI:10.1021/ja052856f

Reference yield: 94.0%

4-bromo-4'-iodobenzophenone (609820-28-2) + ethane-1,2-dithiol (540-63-6) → 2-(4-bromophenyl)-2-(4-iodophenyl)-[1,3]dithiolane (866393-58-0)

Guidance literature:

With BF₃*Ac₂O; In dichloromethane; for 0.333333h;

DOI:10.1021/ja052856f

Reference yield: 71.0%

4-bromo-4'-iodobenzophenone (609820-28-2) + aniline (62-53-3) → (4-bromophenyl)(4-anilinophenyl)methanone

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In toluene; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2012.07.084

upstream raw materials:

(4-bromophenyl)-(4-iodophenyl)methanol

Downstream raw materials:

2-(4-bromophenyl)-2-(4-iodophenyl)-[1,3]dithiolane

{4-[2-(4-bromophenyl)-[1,3]dithiolan-2-yl]phenylethynyl}triisopropylsilane

4-anilino-4'-(4-methylanilino)benzophenone

[4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate