[4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate

Base Information

• Chemical Name: [4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate
• CAS No.: 1448602-20-7
• Molecular Formula: C₇H₇O₃S*C₂₀H₁₅BrIO₂
• Molecular Weight: 665.343
• Mol file: 1448602-20-7.mol

Synonyms:[4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate

Chemical Property of [4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate

There total 1 articles about [4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

4-bromo-4'-iodobenzophenone (609820-28-2) + toluene-4-sulfonic acid (104-15-4) + methoxybenzene (100-66-3) → [4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate (1448602-20-7)

Guidance literature:

4-bromo-4'-iodobenzophenone; With 3-chloro-benzenecarboperoxoic acid; In chloroform;

toluene-4-sulfonic acid; methoxybenzene; In chloroform; at 40 ℃; for 2h;

DOI:10.1039/c3ob40742j

Reference yield: 98.0%

[4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate (1448602-20-7) → [18F]-4-bromo-4′-fluorobenzophenone (1453864-88-4) + [18F]1-fluoro-4-methoxybenzene

Guidance literature:

With K[18F]F-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane complex; In N,N-dimethyl-formamide; at 200 ℃; for 0.0522222h;

DOI:10.1039/c3ob41353e

Reference yield:

[4-(4”-bromophenylcarbonyl)phenyl](4’-methoxyphenyl)tosylate (1448602-20-7) → [18F]-4-bromo-4′-fluorobenzophenone (1453864-88-4)

Guidance literature:

With 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosan/[18F]fluoride; potassium carbonate; In water; N,N-dimethyl-formamide; at 150 ℃; for 0.0502778h; Temperature;

DOI:10.1039/c3ob40742j

upstream raw materials:

4-bromo-4'-iodobenzophenone

toluene-4-sulfonic acid

methoxybenzene

Downstream raw materials:

[¹⁸F]-4-bromo-4′-fluorobenzophenone