N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

Base Information

Chemical Name:N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide
CAS No.:463934-72-7
Molecular Formula:C₃₃H₄₀N₂O₄
Molecular Weight:528.692
Hs Code.:

Synonyms:N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

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Technology Process of N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

There total 1 articles about N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 201677-57-8
N-[2-(benzyloxy)-5-[(2R)-oxiran-2-yl]phenyl]formamide

: N-benzyl-6-(but-3-ynyloxy)hexan-1-amine

: 463934-72-7
N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

Guidance literature:: at 120 ℃; for 2h; Neat (no solvent);
DOI:10.1021/jm801016j

Reference yield: 51.0%

: 463934-72-7
N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

: 50702-39-1
3-iodobenzenesulfonamide

: 463934-73-8
3-(4-{[6-(benzyl{(2R)-2-[4-(benzyloxy)-3-(formylamino)phenyl]-2-hydroxyethyl}amino)hexyl]oxy}but-1-ynyl)benzenesulfonamide

Guidance literature:: With copper(l) iodide; bis(tri-phenylphosphine)palladium(II) dichloride; triethylamine; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm801016j

Reference yield:

: 463934-72-7
N-[5-((1R)-2-{benzyl[6-(but-3-ynyloxy)hexyl]amino}-1-hydroxyethyl)-2-(benzyloxy)phenyl]formamide

: 591-18-4
1-Bromo-3-iodobenzene

: C₃₉H₄₃BrN₂O₄

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) chloride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 48h;