C₂₉H₃₇N₃O₄S₂Si

Base Information

Chemical Name:C₂₉H₃₇N₃O₄S₂Si
CAS No.:1292820-46-2
Molecular Formula:C₂₉H₃₇N₃O₄S₂Si
Molecular Weight:583.848
Hs Code.:

C<sub>29</sub>H<sub>37</sub>N<sub>3</sub>O<sub>4</sub>S<sub>2</sub>Si

Synonyms:C₂₉H₃₇N₃O₄S₂Si

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Chemical Property of C₂₉H₃₇N₃O₄S₂Si

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Technology Process of C₂₉H₃₇N₃O₄S₂Si

There total 5 articles about C₂₉H₃₇N₃O₄S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 690632-17-8
4-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)-1-(triisopropylsilyl)-1H-indole

: 1292820-42-8
C₁₂H₁₁ClN₂O₄S₂

: 1292820-46-2
C₂₉H₃₇N₃O₄S₂Si

Guidance literature:: With chloro(di-2-norbornylphosphino)(2'-dimethylamino-1,1'-biphenyl-2-yl)palladium(II); potassium carbonate; In 1,4-dioxane; at 120 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.01.140

Reference yield:

: 1120-90-7
3-iodopyridine

: 1292820-46-2
C₂₉H₃₇N₃O₄S₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether / toluene

2: sodium tungstate; dihydrogen peroxide

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 1 h / 120 °C / Microwave irradiation; Inert atmosphere

4: chloro(di-2-norbornylphosphino)(2'-dimethylamino-1,1'-biphenyl-2-yl)palladium(II); potassium carbonate / 1,4-dioxane / 1 h / 120 °C / Microwave irradiation; Inert atmosphere

With sodium tungstate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; chloro(di-2-norbornylphosphino)(2'-dimethylamino-1,1'-biphenyl-2-yl)palladium(II); potassium tert-butylate; dihydrogen peroxide; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; bis[2-(diphenylphosphino)phenyl] ether; In 1,4-dioxane; toluene; 3: Buchwald type coupling reaction / 4: Suzuki reaction;
DOI:10.1016/j.tetlet.2011.01.140

Reference yield:

: 915413-21-7
3-(3,5-dichloro-phenylsulfanyl)-pyridine

: 1292820-46-2
C₂₉H₃₇N₃O₄S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tungstate; dihydrogen peroxide

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 1 h / 120 °C / Microwave irradiation; Inert atmosphere

3: chloro(di-2-norbornylphosphino)(2'-dimethylamino-1,1'-biphenyl-2-yl)palladium(II); potassium carbonate / 1,4-dioxane / 1 h / 120 °C / Microwave irradiation; Inert atmosphere

With sodium tungstate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; chloro(di-2-norbornylphosphino)(2'-dimethylamino-1,1'-biphenyl-2-yl)palladium(II); dihydrogen peroxide; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; 2: Buchwald type coupling reaction / 3: Suzuki reaction;
DOI:10.1016/j.tetlet.2011.01.140