1,1-dimethyl-1,2,3,6-tetrahydrosiline

Base Information

Chemical Name:1,1-dimethyl-1,2,3,6-tetrahydrosiline
CAS No.:33546-39-3
Molecular Formula:C₇H₁₄Si
Molecular Weight:126.274
Hs Code.:

Synonyms:1,1-dimethyl-1,2,3,6-tetrahydrosiline

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Chemical Property of 1,1-dimethyl-1,2,3,6-tetrahydrosiline

Chemical Property:

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Technology Process of 1,1-dimethyl-1,2,3,6-tetrahydrosiline

There total 1 articles about 1,1-dimethyl-1,2,3,6-tetrahydrosiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 24171-43-5
allyl(3-butenyl)dimethylsilane

: 33546-39-3
1,1-dimethyl-1,2,3,6-tetrahydrosiline

: 74-85-1
ethene

: 78558-58-4
(E)-1,6-Bis-(allyl-dimethyl-silanyl)-hex-3-ene

: 78558-56-2
4-{[(E)-4-(But-3-enyl-dimethyl-silanyl)-but-2-enyl]-dimethyl-silanyl}-but-1-ene

: 78558-57-3
(E)-5-(Allyl-dimethyl-silanyl)-1-(but-3-enyl-dimethyl-silanyl)-pent-2-ene

Guidance literature:: With tetra-n-butyltin(IV); aluminum oxide; rhenium(VII) oxide; In n-heptane; at 45 ℃; for 3h; Product distribution;
DOI:10.1007/BF00949601

Reference yield: 88.0%

: 33546-39-3
1,1-dimethyl-1,2,3,6-tetrahydrosiline

: 187458-83-9
1,1-dimethyl-1-silacyclohex-3-ene oxide

Guidance literature:: With dihydrogen peroxide; potassium hydrogencarbonate; In methanol; acetonitrile; for 90h; Ambient temperature;
DOI:10.1071/CH9961293

Reference yield:

: 33546-39-3
1,1-dimethyl-1,2,3,6-tetrahydrosiline

: 4-Nitro-benzoic acid (3R,4R)-4-hydroxy-1,1-dimethyl-silinan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / KHCO₃, 30percent H₂O₂ soln. / methanol; acetonitrile / 90 h / Ambient temperature

2: CHCl₃ / 24 h

With dihydrogen peroxide; potassium hydrogencarbonate; In methanol; chloroform; acetonitrile;
DOI:10.1071/CH9961293