4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

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Chemical Name:4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide
CAS No.:1290593-30-4
Molecular Formula:C₃₅H₂₆N₈O₆S₂
Molecular Weight:718.773
Hs Code.:

Synonyms:4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

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Chemical Property of 4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

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Technology Process of 4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

There total 3 articles about 4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1161947-50-7
1-(4-aminophenyl)-4-benzoyl-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazole-2-yl)-1H-pyrazole-3-carboxamide

: 93-91-4
1-phenylbutan-1,3-dione

: 1290593-30-4
4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: 1-(4-aminophenyl)-4-benzoyl-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazole-2-yl)-1H-pyrazole-3-carboxamide; With hydrogenchloride; sodium acetate; sodium nitrite; In water; at 0 - 5 ℃;

1-phenylbutan-1,3-dione; In ethanol; water;
DOI:10.3109/14756366.2010.491795

Reference yield:

: 1100715-17-0
C₂₅H₁₇N₇O₆S₂

: 1290593-30-4
4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodiumsulfide nonahydrate / water

2: hydrogenchloride; sodium acetate; sodium nitrite / water / 0 - 5 °C

With hydrogenchloride; sodiumsulfide nonahydrate; sodium acetate; sodium nitrite; In water;
DOI:10.3109/14756366.2010.491795

Reference yield:

: 658081-76-6
4-benzoyl-1-(4-nitrophenyl)-5-phenyl-1H-pyrazole-3-carboxylic acid

: 1290593-30-4
4-benzoyl-1-(4-(2-(1,3-dioxo-1-phenylbutan-2-ylidene)hydrazinyl)phenyl)-5-phenyl-N-(5-sulphamoyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride

2: hydrogenchloride; sodiumsulfide nonahydrate / water

3: hydrogenchloride; sodium acetate; sodium nitrite / water / 0 - 5 °C

With hydrogenchloride; thionyl chloride; sodiumsulfide nonahydrate; sodium acetate; sodium nitrite; In water;
DOI:10.3109/14756366.2010.491795