4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

Base Information

Chemical Name:4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt
CAS No.:111540-29-5
Molecular Formula:C₁₆H₃₆N*C₁₉H₁₇N₂O₅S
Molecular Weight:627.889
Hs Code.:

Synonyms:4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

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Chemical Property of 4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

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Technology Process of 4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

There total 5 articles about 4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78905-28-9,81767-89-7
cis-3-azido-2-oxo-4-(2-phenylethenyl)-1-azetidine

: 111540-29-5
4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / H₂ / nickel boride / ethanol / 2 h

2: 51 percent / pyridine / CH₂Cl₂ / 3 h / 0 °C

3: 1.) pyridine-sulfur trioxide complex / 1.) pyridine, 80 deg C, 2 h; 2.) CH₂Cl₂

With pyridine; hydrogen; sulfur trioxide pyridine complex; nickel boride; In ethanol; dichloromethane;
DOI:10.1139/v87-014

Reference yield:

: (3S,4R)-3-Azido-1-[bis-(4-methoxy-phenyl)-methyl]-4-((E)-styryl)-azetidin-2-one

: 111540-29-5
4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 0.75 h / -5 - 0 °C

2: 30 percent / H₂ / nickel boride / ethanol / 2 h

3: 51 percent / pyridine / CH₂Cl₂ / 3 h / 0 °C

4: 1.) pyridine-sulfur trioxide complex / 1.) pyridine, 80 deg C, 2 h; 2.) CH₂Cl₂

With pyridine; ammonium cerium(IV) nitrate; hydrogen; sulfur trioxide pyridine complex; nickel boride; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1139/v87-014

Reference yield:

: 82730-15-2
(3R,4S)-3-Amino-4-((E)-styryl)-azetidin-2-one

: 111540-29-5
4-styryl-3-phenylacetamido 2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / pyridine / CH₂Cl₂ / 3 h / 0 °C

2: 1.) pyridine-sulfur trioxide complex / 1.) pyridine, 80 deg C, 2 h; 2.) CH₂Cl₂

With pyridine; sulfur trioxide pyridine complex; In dichloromethane;
DOI:10.1139/v87-014