racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride

Base Information

• Chemical Name: racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride
• CAS No.: 1449220-62-5
• Molecular Formula: C₂₂H₂₈ClNO₂*ClH
• Molecular Weight: 410.384

Synonyms:racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride

Chemical Property of racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride

Chemical Property:

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Technology Process of racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride

There total 1 articles about racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoic acid (1076199-77-3) → racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride (1449220-62-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In ethyl acetate;

Reference yield: 35.0%

(-)-menthol (2216-51-5) + racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride (1449220-62-5) → L-(-)-menthyl 3-(3-N,N'-diisopropylamino-1(S)-phenyl-propyl)-4-hydroxy-benzoate hydrochloride (1449220-63-6) + L-(-)-menthyl 3-(3-N,N'-diisopropylamino-1(R)-phenyl-propyl)-4-hydroxy-benzoate hydrochloride

Guidance literature:

In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

Reference yield: 35.0%

(1S,2R,5S)-(+)-menthol (15356-60-2) + racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoyl chloride hydrochloride (1449220-62-5) → D-(+)-menthyl 3-(3-N,N'-diisopropylamino-1(R)-phenyl-propyl)-4-hydroxy-benzoate hydrochloride (1449220-60-3) + D-(+)-menthyl 3-(3-N,N'-diisopropylamino-1(S)-phenyl-propyl)-4-hydroxy-benzoate hydrochloride

Guidance literature:

In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

upstream raw materials:

racemic 3-(3-N,N'-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoic acid

Downstream raw materials:

D-(+)-menthyl 3-(3-N,N'-diisopropylamino-1(R)-phenyl-propyl)-4-hydroxy-benzoate hydrochloride

Tolterodine acid

(R)-3-(N,N'-diisopropylamino-1-phenyl-propyl)-4-isobutyryloxy-benzoic acid

fesoterodine

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