2,3-Dichloro-α-(2,3-dichloro-4-Methoxyphenyl)-4-Methoxy-benzeneacetic Acid Ethyl Ester

Base Information

• Chemical Name: 2,3-Dichloro-α-(2,3-dichloro-4-Methoxyphenyl)-4-Methoxy-benzeneacetic Acid Ethyl Ester
• CAS No.: 316382-53-3
• Molecular Formula: C₁₈H₁₆Cl₄O₄
• Molecular Weight: 438.135
• Mol file: 316382-53-3.mol

Synonyms:bis-(2,3-dichloro-4-methoxy-phenyl)-acetic acid ethyl ester

Chemical Property of 2,3-Dichloro-α-(2,3-dichloro-4-Methoxyphenyl)-4-Methoxy-benzeneacetic Acid Ethyl Ester

Chemical Property:

• Boiling Point: 503.2±50.0 °C(Predicted)
• Density: 1.376±0.06 g/cm3(Predicted)
• Solubility.: Chloroform, Dichloromethane

Purity/Quality:

99% ^*data from raw suppliers

2,3-Dichloro-α-(2,3-dichloro-4-methoxyphenyl)-4-methoxy-benzeneaceticAcidEthylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2,3-Dichloro-α-(2,3-dichloro-4-methoxyphenyl)-4-methoxy-benzeneacetic Acid Ethyl Ester is an intermediate in the preparation of ethylidenebisaripiprazole.

Technology Process of 2,3-Dichloro-α-(2,3-dichloro-4-Methoxyphenyl)-4-Methoxy-benzeneacetic Acid Ethyl Ester

There total 2 articles about 2,3-Dichloro-α-(2,3-dichloro-4-Methoxyphenyl)-4-Methoxy-benzeneacetic Acid Ethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,3-dichloroanisole (1984-59-4) + ethyl glyoxylate polymer → bis-(2,3-dichloro-4-methoxy-phenyl)-acetic acid ethyl ester (316382-53-3)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; Heating;

DOI:10.1016/S0960-894X(02)00857-0

Reference yield:

glyoxylic acid ethyl ester (924-44-7) + 2,3-dichloroanisole (1984-59-4) → bis-(2,3-dichloro-4-methoxy-phenyl)-acetic acid ethyl ester (316382-53-3)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; at 110 - 135 ℃; for 2h;

DOI:10.1016/S0968-0896(02)00110-4

Reference yield: 100.0%

bis-(2,3-dichloro-4-methoxy-phenyl)-acetic acid ethyl ester (316382-53-3) → 2,2-bis-(2,3-dichloro-4-methoxy-phenyl)-ethanol (476014-22-9)

Guidance literature:

With sodium tetrahydroborate; zirconium(IV) chloride;

DOI:10.1016/S0960-894X(02)00857-0

upstream raw materials:

glyoxylic acid ethyl ester

2,3-dichloroanisole

Downstream raw materials:

2,2-bis-(2,3-dichloro-4-methoxy-phenyl)-ethanol

C₁₆H₁₃BrCl₄O₂

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