2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl

Base Information

• Chemical Name: 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl
• CAS No.: 84379-29-3
• Molecular Formula: C₃₈H₄₄Br₂N₄O₅
• Molecular Weight: 796.599

Synonyms:2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl

Chemical Property of 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl

Chemical Property:

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Technology Process of 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl

There total 5 articles about 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-28-2) → 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-29-3)

Guidance literature:

Multi-step reaction with 2 steps

2: base

With base;

DOI:10.1039/c39820001219

Reference yield:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-27-1) → 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-29-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 68 percent / metallation

3: base

With base;

DOI:10.1039/c39820001219

Reference yield:

3-bromopropylamine hydrochloride (5003-71-4) + 2'-Benzyloxy-3,3''-diisocyanato-2,2''-dimethoxy-5,5',5''-trimethyl-[1,1';3',1'']terphenyl → 2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis<3-(3-bromopropyl)ureido>5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-29-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In toluene;

DOI:10.1021/ja00335a049

upstream raw materials:

3-bromopropylamine hydrochloride

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dibromo-5,5',5''-trimethyl-1,1':3',1''-terphenyl

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl

Downstream raw materials:

34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-bis(hexahydro-2-oxopyrimidinyl)-1,1':3',1''-terphenyl

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