C₅₀H₄₉ClO₆

Base Information

Chemical Name:C₅₀H₄₉ClO₆
CAS No.:1413373-26-8
Molecular Formula:C₅₀H₄₉ClO₆
Molecular Weight:781.388
Hs Code.:

C<sub>50</sub>H<sub>49</sub>ClO<sub>6</sub>

Synonyms:C₅₀H₄₉ClO₆

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Chemical Property of C₅₀H₄₉ClO₆

Chemical Property:

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Technology Process of C₅₀H₄₉ClO₆

There total 12 articles about C₅₀H₄₉ClO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1161430-56-3
C₅₀H₅₁ClO₆

: 1413373-26-8
C₅₀H₄₉ClO₆

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-26-8
C₅₀H₄₉ClO₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

5.2: 3 h / 25 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Reflux

7.2: 0 °C

7.3: 25 - 30 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; triethylsilane; oxalyl dichloride; dimethylsulfide borane complex; boron trifluoride diethyl etherate; Dess-Martin periodane; magnesium; dimethyl sulfoxide; L-proline; trichlorophosphate; ethylene dibromide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 110391-10-1
(4R,5S,6R)-4,5,6-tris(benzyloxy)-3-((benzyloxy)methyl)-2-cyclohexen-1-one

: 1413373-26-8
C₅₀H₄₉ClO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

1.2: 3 h / 25 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

3.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Reflux

3.2: 0 °C

3.3: 25 - 30 °C

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With triethylsilane; dimethylsulfide borane complex; boron trifluoride diethyl etherate; Dess-Martin periodane; magnesium; ethylene dibromide; In tetrahydrofuran; dichloromethane;