Technology Process of C44H59NO10
There total 6 articles about C44H59NO10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; di(n-butyl)tin oxide;
In
toluene;
at 110 ℃;
for 2h;
Inert atmosphere;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1.5 h / 110 °C / Inert atmosphere
2.1: sodium methylate / methanol / 4 h / 20 °C / Inert atmosphere
2.2: Amberlite IR120 H+ resin
3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
4.1: di(n-butyl)tin oxide; tetrabutylammomium bromide / toluene / 2 h / 110 °C / Inert atmosphere; Molecular sieve
With
2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
methanol; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium methylate / methanol / 4 h / 20 °C / Inert atmosphere
1.2: Amberlite IR120 H+ resin
2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
3.1: di(n-butyl)tin oxide; tetrabutylammomium bromide / toluene / 2 h / 110 °C / Inert atmosphere; Molecular sieve
With
tetrabutylammomium bromide; sodium methylate; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
methanol; N,N-dimethyl-formamide; toluene;
