N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide
CAS No.:260782-35-2
Molecular Formula:C₁₉H₃₁NO₇
Molecular Weight:385.458
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

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Chemical Property of N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

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Technology Process of N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

There total 3 articles about N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 132415-06-6
5-(((1-cyclohexyl)hydroxy)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 260782-35-2
N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

Guidance literature:: In toluene; at 65 ℃; for 4h;
DOI:10.1021/jo991409d

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 260782-35-2
N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

2: 91 percent / toluene / 4 h / 65 °C

With pyridine; In dichloromethane; toluene; 1: Acylation / 2: Substitution;
DOI:10.1021/jo991409d

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 260782-35-2
N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-4-cyclohexyl-3-oxopropionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / diethyl cyanophosphonate; Et₃N / dimethylformamide / 0 - 20 °C

2: 91 percent / toluene / 4 h / 65 °C

With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; toluene; 1: Acylation / 2: Substitution;
DOI:10.1021/jo991409d