N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

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Chemical Name:N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide
CAS No.:86955-55-7
Molecular Formula:C₃₂H₅₂N₂O₁₀S₂
Molecular Weight:688.904
Hs Code.:

N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

Synonyms:N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

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Chemical Property of N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

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Technology Process of N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

There total 8 articles about N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 72223-72-4
(2S)-3-<(1-methylethyl)(methylsulfonyl)amino>-1-<(methylsulfonyl)oxy>-2-propanol

: 86955-51-3
C₁₈H₂₂O₄

: 86955-55-7
N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; at 80 ℃; for 6h;
DOI:10.1021/jm00365a004

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 86955-55-7
N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 4 N NaOH / dimethylsulfoxide / 1 h / 75 °C

2: 82 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Heating

3: 76 percent / 4 N NaOH / dimethylsulfoxide / 6 h / 80 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dimethyl sulfoxide;
DOI:10.1021/jm00365a004

Reference yield:

: 6272-38-4
O-benzylcatechol

: 86955-55-7
N-{(S)-2-Hydroxy-3-[2-(6-{2-[(S)-2-hydroxy-3-(isopropyl-methanesulfonyl-amino)-propoxy]-phenoxy}-hexyloxy)-phenoxy]-propyl}-N-isopropyl-methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 4 N NaOH / dimethylsulfoxide / 1 h / 75 °C

2: 82 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Heating

3: 76 percent / 4 N NaOH / dimethylsulfoxide / 6 h / 80 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dimethyl sulfoxide;
DOI:10.1021/jm00365a004