carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester

Base Information

• Chemical Name: carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester
• CAS No.: 1394141-21-9
• Molecular Formula: C₂₆H₂₈N₆O₇
• Molecular Weight: 536.544
• Mol file: 1394141-21-9.mol

Synonyms:carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester

Chemical Property of carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester

There total 2 articles about carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

dihydrozeatin (23599-75-9) + imidazole-1-carboxylic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester (1394141-19-5) → carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester (1394141-21-9)

Guidance literature:

With caesium carbonate; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2012.06.090

Reference yield:

2,5-dimethoxyphenylmagnesium bromide (62890-98-6) → carbonic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester 2-methyl-4-(9H-purin-6-ylamino)butyl ester (1394141-21-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 2 h / -78 - 0 °C

2: dichloromethane / 1 h / 20 °C

3: caesium carbonate / tetrahydrofuran / 20 °C

With caesium carbonate; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2012.06.090

upstream raw materials:

dihydrozeatin

imidazole-1-carboxylic acid (2,5-dimethoxyphenyl)(2-nitrophenyl)methyl ester

2,5-dimethoxyphenylmagnesium bromide