C₁₆H₁₂BrF₃O₄

Base Information

Chemical Name:C₁₆H₁₂BrF₃O₄
CAS No.:1359024-92-2
Molecular Formula:C₁₆H₁₂BrF₃O₄
Molecular Weight:405.168
Hs Code.:

C<sub>16</sub>H<sub>12</sub>BrF<sub>3</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₂BrF₃O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₂BrF₃O₄

Chemical Property:

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Technology Process of C₁₆H₁₂BrF₃O₄

There total 8 articles about C₁₆H₁₂BrF₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1359024-91-1
C₁₅H₁₀BrF₃O₄

: 74-88-4
methyl iodide

: 1359024-92-2
C₁₆H₁₂BrF₃O₄

Guidance literature:: C₁₅H₁₀BrF₃O₄; With n-butyllithium; Di-sec-butylamin; N,N,N,N,-tetramethylethylenediamine; triethylamine hydrochloride; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.01667h;

With ammonium chloride; In tetrahydrofuran; hexane; water;

Reference yield:

: 660848-57-7
2-methoxy-5-(trifluoromethoxy)aniline

: 1359024-92-2
C₁₆H₁₂BrF₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium hydrobromide perbromide

2: hydrogenchloride; sodium nitrite

3: TurboGrignard

4: LiN(i-C₄H₉)2; N,N,N,N,-tetramethylethylenediamine

With hydrogenchloride; TurboGrignard; pyridinium hydrobromide perbromide; LiN(i-C₄H₉)2; N,N,N,N,-tetramethylethylenediamine; sodium nitrite;
DOI:10.1021/acs.jmedchem.6b01903

Reference yield:

: 710-18-9
1-methoxy-4-(trifluoromethoxy)benzene

: 1359024-92-2
C₁₆H₁₂BrF₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1: nitric acid; sulfuric acid

2: sodium dithionite

3: pyridinium hydrobromide perbromide

4: hydrogenchloride; sodium nitrite

5: TurboGrignard

6: LiN(i-C₄H₉)2; N,N,N,N,-tetramethylethylenediamine

With hydrogenchloride; TurboGrignard; sodium dithionite; pyridinium hydrobromide perbromide; LiN(i-C₄H₉)2; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; nitric acid; sodium nitrite;
DOI:10.1021/acs.jmedchem.6b01903