2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

Base Information

Chemical Name:2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide
CAS No.:1402063-74-4
Molecular Formula:C₁₉H₂₁O₃P
Molecular Weight:328.348
Hs Code.:

Synonyms:2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

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Chemical Property of 2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

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Technology Process of 2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

There total 3 articles about 2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1402063-56-2
4-chloro-2-ethoxy-2,5-dihydro-5,5-dimethyl-3-phenyl-1,2-oxaphosphole 2-oxide

: 98-80-6
phenylboronic acid

: 1402063-74-4
2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

Guidance literature:: With C₄₂H₆₆Cl₂O₆P₂Pd; potassium carbonate; In toluene; for 17h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201200228

Reference yield:

: 195318-34-4
diethyl (3-methyl-1-phenylbuta-1,2-dien-1-yl)phosphonate

: 1402063-74-4
2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) choride dihydrate / toluene / 24 h / 70 °C

2: C₄₂H₆₆Cl₂O₆P₂Pd; potassium carbonate / toluene / 17 h / Inert atmosphere; Reflux

With copper(II) choride dihydrate; C₄₂H₆₆Cl₂O₆P₂Pd; potassium carbonate; In toluene; 2: Suzuki coupling;
DOI:10.1002/ejoc.201200228

Reference yield:

: 1719-19-3
2-Methyl-4-phenyl-3-butyn-2-ol

: 1402063-74-4
2-ethoxy-2,5-dihydro-5,5-dimethyl-3,4-diphenyl-1,2-oxaphosphole 2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / -78 - 20 °C

2: copper(II) choride dihydrate / toluene / 24 h / 70 °C

3: C₄₂H₆₆Cl₂O₆P₂Pd; potassium carbonate / toluene / 17 h / Inert atmosphere; Reflux

With copper(II) choride dihydrate; C₄₂H₆₆Cl₂O₆P₂Pd; potassium carbonate; triethylamine; In dichloromethane; toluene; 1: Claisen rearrangement / 3: Suzuki coupling;
DOI:10.1002/ejoc.201200228