1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea

Base Information

• Chemical Name: 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea
• CAS No.: 1038963-55-1
• Molecular Formula: C₂₂H₂₉Cl₂N₅O₂
• Molecular Weight: 466.411

Synonyms:1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea

Chemical Property of 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea

Chemical Property:

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Technology Process of 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea

There total 2 articles about 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[3-(4-(bis(2-chloroethyl)amino)phenyl)ureido]benzoic acid (1262789-83-2) + N,N-dimethylethylenediamine (108-00-9) → 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea (1038963-55-1)

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

DOI:10.1016/j.bmc.2010.11.005

Reference yield:

1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea hydrochloride (1038623-53-8) → 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea (1038963-55-1)

Guidance literature:

With sodium hydrogencarbonate; In water; pH=7 - 8;

DOI:10.1016/j.bmc.2010.11.005

Reference yield:

1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea (1038963-55-1) → 1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea hydrochloride (1038623-53-8)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 ℃;

DOI:10.1016/j.bmc.2010.11.005

upstream raw materials:

3-[3-(4-(bis(2-chloroethyl)amino)phenyl)ureido]benzoic acid

N,N-dimethylethylenediamine

1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea hydrochloride

Downstream raw materials:

1-[3-((2-(dimethylamino)ethyl)carbamoyl)phenyl]-3-[4-(bis(2-chloroethyl)amino)-phenyl]urea hydrochloride

CH₄O₃S*C₂₂H₂₉Cl₂N₅O₂

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