biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

Base Information

Chemical Name:biacethyl-2-oxime-3-p-nitrobenzoylhydrazone
CAS No.:90054-17-4
Molecular Formula:C₁₁H₁₂N₄O₄
Molecular Weight:264.241
Hs Code.:

Synonyms:biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

Suppliers and Price of biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

There total 1 articles about biacethyl-2-oxime-3-p-nitrobenzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 636-97-5
N-amino-(4-nitrophenyl)carboxamide

: 135636-66-7
butane-2,3-dione mono-oxime

: 90054-17-4
biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

Guidance literature:: In methanol; Yield given; Ambient temperature;
DOI:10.1039/P19890000619

Reference yield: 70.0%

: 6018-89-9
nickel(II) acetate tetrahydrate

: 90054-17-4
biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

: [Ni(ONC(CH₃)C(CH₃)NNHC(O)(p-O₂NC₆H₄))]2*3H₂O

Guidance literature:: With KOH; In ethanol; 1 equiv. of ethanolic soln. of Ni-salt was added to EtOH soln. of N-compd., 2 equiv. of KOH was added in EtOH, reflux for 3 h; ppt. was filtered off, washed several times with EtOH, dried in vac., elem. anal.;
DOI:10.1016/j.poly.2007.05.010

Reference yield: 68.0%

: copper(II) chloride hydrate

: 90054-17-4
biacethyl-2-oxime-3-p-nitrobenzoylhydrazone

: 89952-88-5
[(biacethyl-2-oximo-3-p-nitrobenzoylhydrazone)-dichloro-copper]

Guidance literature:: In ethanol; ligand mixed in molar ratio 1/1 with hydrated metal salt in abs. EtOH, heated on H2O bath for 1 h; filtered off, washed with EtOH, then with Et2O, dried (vac.) over CaCl2; elem. anal.;