6--4-chloropyrimidine

Base Information

• Chemical Name: 6--4-chloropyrimidine
• CAS No.: 155670-20-5
• Molecular Formula: C₁₃H₁₂ClN₃O₂
• Molecular Weight: 277.71

Synonyms:6--4-chloropyrimidine

Chemical Property of 6--4-chloropyrimidine

Chemical Property:

Purity/Quality:

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Technology Process of 6--4-chloropyrimidine

There total 1 articles about 6--4-chloropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.2%

4,6-dichloropyrimidine (1193-21-1) + N-benzylglycine sodium salt → 6--4-chloropyrimidine (155670-20-5)

Guidance literature:

In ethanol; Heating;

DOI:10.1021/jo00088a031

Reference yield: 94.6%

sodium methylate (124-41-4) + 6--4-chloropyrimidine (155670-20-5) → 6--4-methoxypyrimidine (155670-21-6)

Guidance literature:

In methanol; for 24h; Heating;

DOI:10.1021/jo00088a031

Reference yield: 55.0%

6--4-chloropyrimidine (155670-20-5) + trifluoroacetic anhydride (407-25-0) → 1-Benzyl-7-chloro-2-(trifluoroacetyl)imidazo<1,2-c>pyrimidin-3-one

Guidance literature:

With triethylamine; In dichloromethane; 1.) -78 deg C, 10 min, 2.) -78 deg C to r.t., 20 min;

DOI:10.1021/jo00088a031

upstream raw materials:

4,6-dichloropyrimidine

Downstream raw materials:

6--4-methoxypyrimidine

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