Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

Base Information

Chemical Name:Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside
CAS No.:120016-85-5
Molecular Formula:C₁₅H₁₇N₃O₅
Molecular Weight:319.317
Hs Code.:

Synonyms:Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

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Chemical Property of Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

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Technology Process of Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

There total 3 articles about Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: Methyl 4,6-O-benzylidene-2-deoxy-3,3'-epoxy-3'-(p-tolylsulfonyl)-α-D-ribo-hexopyranoside

: 120016-85-5
Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 4h;

Reference yield: 75.0%

: C₂₂H₂₄O₇S

: 120016-85-5
Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

Guidance literature:: With sodium azide; potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol; for 3h; Ambient temperature;
DOI:10.1039/c39880001581

Reference yield:

: 6752-49-4
(4aR,6S,8aR)-6-Methoxy-2-phenyl-tetrahydro-pyrano[3,2-d][1,3]dioxin-8-one

: 120016-85-5
Methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 3 h / Ambient temperature

2: 78 percent / NaN₃ / dimethylformamide / 4 h / 80 °C

With sodium azide; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;