(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

Base Information

Chemical Name:(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide
CAS No.:128269-65-8
Molecular Formula:C₁₆H₂₄N₂O₃
Molecular Weight:292.378
Hs Code.:

Synonyms:(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

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Chemical Property of (2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

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Technology Process of (2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

There total 6 articles about (2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 128257-12-5
(3aS,6R)-6-(2-Methoxyphenyl)-5-oxa-7,8a-diazaperhydroazulen-8-one

: 557-20-0
diethylzinc

: 128269-65-8
(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

Guidance literature:: In toluene; at 0 ℃; for 3h;
DOI:10.3987/COM-89-S35

Reference yield:

: 128257-10-3,578740-87-1
(S)-1-carbamoyl-2-hydroxymethylpyrrolidine

: 128269-65-8
(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / p-toluenesulfonic acid monohydrate / toluene / Heating

2: diethyl ether; tetrahydrofuran / 3 h / 0 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1248/cpb.38.2627

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 128269-65-8
(2S,1'S)-2-Hydroxymethyl-N-1'-(2-methoxyphenyl)propyl-1-pyrrolidinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / p-toluenesulfonic acid monohydrate / toluene / Heating

2: diethyl ether; tetrahydrofuran / 3 h / 0 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1248/cpb.38.2627