5-Amino-3-bromo-2-nitrobenzoic acid

Base Information

Chemical Name:5-Amino-3-bromo-2-nitrobenzoic acid
CAS No.:60912-51-8
Molecular Formula:C7H5BrN2O4
Molecular Weight:261.03
Hs Code.:2922499990
DSSTox Substance ID:DTXSID60415419
Wikidata:Q82224343
Mol file:60912-51-8.mol

Synonyms:5-amino-3-bromo-2-nitrobenzoic acid;60912-51-8;Benzoic acid,5-amino-3-bromo-2-nitro-;DTXSID60415419;FT-0709133

Suppliers and Price of 5-Amino-3-bromo-2-nitrobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-AMINO-3-BROMO-2-NITRO-BENZOICACID 95.00%
5MG
$ 504.04

Total 9 raw suppliers

Chemical Property of 5-Amino-3-bromo-2-nitrobenzoic acid

Chemical Property:

Vapor Pressure:1.45E-09mmHg at 25°C
Refractive Index:1.709
Boiling Point:468.1 °C at 760 mmHg
Flash Point:236.9 °C
PSA：109.14000
Density:1.973 g/cm³
LogP:2.74210
XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:259.94327
Heavy Atom Count:14
Complexity:255

Purity/Quality:

98%Min ^*data from raw suppliers

5-AMINO-3-BROMO-2-NITRO-BENZOICACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1C(=O)O)[N+](=O)[O-])Br)N

Technology Process of 5-Amino-3-bromo-2-nitrobenzoic acid

There total 5 articles about 5-Amino-3-bromo-2-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 54002-33-4
methyl 3-bromo-2-nitro-5-acetylaminobenzoate

: 60912-51-8
3-Bromo-2-nitro-5-amino-benzoesaeure

Guidance literature:: With water; barium(II) hydroxide; In methanol; for 18h; Reflux;
DOI:10.1016/j.mencom.2020.11.006

Reference yield:

: 42237-85-4
3-amino-5-bromobenzoic acid

: 60912-51-8
3-Bromo-2-nitro-5-amino-benzoesaeure

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 2 h / 0 - 25 °C / Reflux

2: triethylamine; dmap / tetrahydrofuran / 25 °C

3: nitric acid; sulfuric acid / 0.5 h / 0 - 25 °C

4: barium(II) hydroxide; water / methanol / 18 h / Reflux

With dmap; thionyl chloride; sulfuric acid; water; nitric acid; triethylamine; barium(II) hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.mencom.2020.11.006

Reference yield:

: 706791-83-5
3-amino-5-bromobenzoic acid methyl ester

: 60912-51-8
3-Bromo-2-nitro-5-amino-benzoesaeure

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dmap / tetrahydrofuran / 25 °C

2: nitric acid; sulfuric acid / 0.5 h / 0 - 25 °C

3: barium(II) hydroxide; water / methanol / 18 h / Reflux

With dmap; sulfuric acid; water; nitric acid; triethylamine; barium(II) hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.mencom.2020.11.006