prop-2-ynyl 4-phenylbutyrate

Base Information

• Chemical Name: prop-2-ynyl 4-phenylbutyrate
• CAS No.: 1180629-83-7
• Molecular Formula: C₁₃H₁₄O₂
• Molecular Weight: 202.253
• Mol file: 1180629-83-7.mol

Synonyms:prop-2-ynyl 4-phenylbutyrate

Chemical Property of prop-2-ynyl 4-phenylbutyrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of prop-2-ynyl 4-phenylbutyrate

There total 1 articles about prop-2-ynyl 4-phenylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

propargyl alcohol (107-19-7) + 4-Phenylbutyric acid (1821-12-1) → prop-2-ynyl 4-phenylbutyrate (1180629-83-7)

Guidance literature:

With silica gel-immobilized perchloric acid; at 80 ℃; for 6h; Inert atmosphere; Neat (no solvent);

DOI:10.1021/jo900614s

Reference yield: 86.0%

4-toluenesulfonyl azide (941-55-9) + prop-2-ynyl 4-phenylbutyrate (1180629-83-7) → (1-tosyl-1H-1,2,3-triazol-4-yl)methyl 4-phenylbutanoate

Guidance literature:

With copper(I) thiophene-2-carboxylate; In toluene; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/adsc.202000632

upstream raw materials:

propargyl alcohol

4-Phenylbutyric acid