sodium bis(2-mercapto-p-tolylimidazolyl)borate

Base Information

Chemical Name:sodium bis(2-mercapto-p-tolylimidazolyl)borate
CAS No.:511534-90-0
Molecular Formula:C₂₀H₂₀BN₄S₂*Na
Molecular Weight:414.338
Hs Code.:

Synonyms:sodium bis(2-mercapto-p-tolylimidazolyl)borate

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Chemical Property of sodium bis(2-mercapto-p-tolylimidazolyl)borate

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Technology Process of sodium bis(2-mercapto-p-tolylimidazolyl)borate

There total 1 articles about sodium bis(2-mercapto-p-tolylimidazolyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 16940-66-2
sodium tetrahydroborate

: 23671-38-7
1-(4-methylphenyl)imidazole-2-thione

: 511534-90-0
sodium bis(2-mercapto-p-tolylimidazolyl)borate

Guidance literature:: In tetrahydrofuran; Ar; refluxing of THF suspn. of NaBH4 with 2 equivs. of ligand for 20 h, cooling to room temp.; filtration, concg. the filtrate under reduced pressure, trituration withpentane for 2 h, filtration, washing with pentane, drying in vac. for 3 h;
DOI:10.1021/ic025780m

Reference yield: 85.0%

: 511534-90-0
sodium bis(2-mercapto-p-tolylimidazolyl)borate

: [RuHCl(CO)(PPh₃)₃]

: C₃₉H₃₆BN₄OPRuS₂

Guidance literature:: In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.06.017

Reference yield: 68.0%

: 511534-90-0
sodium bis(2-mercapto-p-tolylimidazolyl)borate

: 10108-64-2
cadmium(II) chloride

: 511534-85-3
cadmium(II) bis(2-mercapto-p-tolylimidazolyl)borate

Guidance literature:: In methanol; water; byproducts: NaCl; treating of aq. soln. of CdCl2 with 2 equivs. of borate dissolved in methanol, stirring the suspn. for 15 min; filtration, drying the solid in vac. for 3 h; elem. anal.;
DOI:10.1021/ic025780m