(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

Base Information

Chemical Name:(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride
CAS No.:1204110-70-2
Molecular Formula:C₃₁H₂₇N₄O₂*Cl
Molecular Weight:523.034
Hs Code.:

Synonyms:(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

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Chemical Property of (E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

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Technology Process of (E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

There total 1 articles about (E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 136152-26-6
1,3,4-triphenyl-1,2,4-triazolium chloride

: 1093279-83-4
methyl 2-methyl-3-(phenylimino)acrylate

: 1204110-70-2
(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

Guidance literature:: 1,3,4-triphenyl-1,2,4-triazolium chloride; With potassium tert-butylate; In tetrahydrofuran; at -20 ℃; for 0.0833333h; Inert atmosphere;

methyl 2-methyl-3-(phenylimino)acrylate; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b915215f

Reference yield: 71.0%

: 1204110-70-2
(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

: 762-42-5
dimethyl acetylenedicarboxylate

: 1204135-54-5
(E)-dimethyl 2'-(1-methoxycarbonylethylidene)-1,1'3,4-tetraphenyl-1,1',2',4-tetrahydrospiro[1,2,4-triazole-2,3'-pyrrole]-4',5'-dicarboxylate

Guidance literature:: (E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride; With potassium tert-butylate; In toluene; at 20 - 80 ℃; Inert atmosphere;

dimethyl acetylenedicarboxylate; In toluene; at 80 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b915215f

Reference yield: 49.0%

: 1017684-70-6
C₇H₁₀O₂

: 1204110-70-2
(E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride

: (2'E,5'E,3'RS,4'RS)-methyl 2'-(1-methoxycarbonylethylidene)-1,1',3,4-tetraphenyl-5'-propylidene-1,4-dihydrospiro[1,2,4-triazole-2,3'-pyrrolidine]-4'-carboxylate

: (2'E,5'E,3'SR,4'RS)-methyl 2'-(1-methoxycarbonylethylidene)-1,1',3,4-tetraphenyl-5'-propylidene-1,4-dihydrospiro[1,2,4-triazole-2,3'-pyrrolidine]-4'-carboxylate

Guidance literature:: (E)-5-(2-methoxycarbonyl-1-phenylamino-1-propenyl)-1,3,4-triphenyl-1,2,4-triazolium chloride; With potassium tert-butylate; In toluene; at 20 - 60 ℃; Inert atmosphere;

C₇H₁₀O₂; In toluene; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1039/b915215f