K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

Base Information

• Chemical Name: K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]
• CAS No.: 203789-81-5
• Molecular Formula: C₁₄H₁₆N₂NiO₂S₂*C₂₄H₂₀P*K
• Molecular Weight: 745.61

Synonyms:K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

Chemical Property of K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

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Technology Process of K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

There total 1 articles about K⁽¹⁺⁾*P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(2-) = K[P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nickel(II) acetate tetrahydrate (6018-89-9) + tetraphenyl phosphonium chloride (2001-45-8) + thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester (186357-20-0) + potassium hydroxide → 2P(C6H5)4(1+)*Ni(C6H4(NCOC(CH3)2S)2)(2-) = [P(C6H5)4]2[Ni(C6H4(NCOC(CH3)2S)2)] + K(1+)*P(C6H5)4(1+)*Ni(C6H4(NCOC(CH3)2S)2)(2-) = K[P(C6H5)4][Ni(C6H4(NCOC(CH3)2S)2)] (203789-81-5)

Guidance literature:

In ethanol; (anaerobic conditions); stirring the org. substrate, KOH and Ph4PCl in EtOH for 30 min, addn. of the Ni salt in EtOH, short reflux;

Reference yield: 54.0%

2P(C6H5)4(1+)*Ni(C6H4(NCOC(CH3)2S)2)(2-) = [P(C6H5)4]2[Ni(C6H4(NCOC(CH3)2S)2)] + K(1+)*P(C6H5)4(1+)*Ni(C6H4(NCOC(CH3)2S)2)(2-) = K[P(C6H5)4][Ni(C6H4(NCOC(CH3)2S)2)] (203789-81-5) → P(C6H5)4(1+)*Ni(C6H4(NCOC(CH3)2S)2)(1-) = [P(C6H5)4][Ni(C6H4(NCOC(CH3)2S)2)] (203789-83-7)

Guidance literature:

With (PPh₄)Cl; In acetonitrile; Electrolysis; exhaustive electrolysis at -0.51 V (Pt net electrode); pptn. of the electrolyte by addn. of Et2O, filtration, removal of solvent, redissoln. (acetone, under N2), crystn. on diffusion of Et2O into this soln.; elem. anal.;

upstream raw materials:

nickel(II) acetate tetrahydrate

tetraphenyl phosphonium chloride

thioacetic acid S-{1-[2-(2-acetylsulfanyl-2-methylpropionylamino)phenylcarbamoyl]-1-methylethyl} ester

Downstream raw materials:

P(C₆H₅)4⁽¹⁺⁾*Ni(C₆H₄(NCOC(CH₃)2S)2)^(1-) = [P(C₆H₅)4][Ni(C₆H₄(NCOC(CH₃)2S)2)]

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