p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

Base Information

Chemical Name:p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid
CAS No.:203632-45-5
Molecular Formula:C₂₄H₂₈O₈
Molecular Weight:444.482
Hs Code.:

Synonyms:p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

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Chemical Property of p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

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Technology Process of p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

There total 8 articles about p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 203632-44-4
p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranoside

: 203632-45-5
p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; for 20h; Ambient temperature;
DOI:10.1021/jo971323p

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3,5,6-di-O-isopropylidene-D-mannofuranose

: 203632-45-5
p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / NaH / dimethylformamide / 24 h / Ambient temperature

2: 93 percent / AcOH / H₂O / 18 h / Ambient temperature

3: 86 percent / imidazole / dimethylformamide / 6 h / Ambient temperature

4: 79 percent / NaH / dimethylformamide / 10 h / Ambient temperature

5: 91 percent / NH₄F / methanol / 20 h / Ambient temperature

6: 70 percent / PDC / dimethylformamide / 20 h / Ambient temperature

With 1H-imidazole; ammonium fluoride; dipyridinium dichromate; sodium hydride; acetic acid; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo971323p

Reference yield:

: 100-39-0
benzyl bromide

: 203632-45-5
p-methoxybenzyl 5-O-benzyl-2,3-O-isopropylidene-α-D-mannofuranosiduronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaH / dimethylformamide / 10 h / Ambient temperature

2: 91 percent / NH₄F / methanol / 20 h / Ambient temperature

3: 70 percent / PDC / dimethylformamide / 20 h / Ambient temperature

With ammonium fluoride; dipyridinium dichromate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo971323p