N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester

Base Information

Chemical Name:N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester
CAS No.:56724-14-2
Molecular Formula:C₁₉H₂₁NO₅
Molecular Weight:343.379
Hs Code.:
DSSTox Substance ID:DTXSID501232366

Synonyms:N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester;DTXSID501232366;56724-14-2

Suppliers and Price of N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:343.14197277
Heavy Atom Count:25
Complexity:424

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=CC(=C1)CC(C(=O)OC)NC(=O)C2=CC=CC=C2)OC

Technology Process of N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester

There total 4 articles about N-Benzoyl-3,5-dimethoxyphenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 295803-57-5
methyl 2-benzoylamino-3-(3,5-dimethoxyphenyl)-2-propenoate

: 56724-14-2
methyl 2-benzoylamino-3-(3,5-dimethoxyphenyl)propanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic acid; for 10h; under 3102.89 Torr;
DOI:10.1016/S0040-4020(00)00470-1

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 56724-14-2
methyl 2-benzoylamino-3-(3,5-dimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / sodium acetate / acetic anhydride / 2.5 h / 85 °C

2: 88 percent / Na₂CO₃ / 0.75 h / Heating

3: H₂ / 10 percent Pd/C / tetrahydrofuran; methanol; acetic acid / 10 h / 3102.89 Torr

With hydrogen; sodium acetate; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic anhydride; acetic acid; 1: Condensation / 2: Ring cleavage / 3: Catalytic hydrogenation;
DOI:10.1016/S0040-4020(00)00470-1

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 56724-14-2
methyl 2-benzoylamino-3-(3,5-dimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / sodium acetate / acetic anhydride / 2.5 h / 85 °C

2: 88 percent / Na₂CO₃ / 0.75 h / Heating

3: H₂ / 10 percent Pd/C / tetrahydrofuran; methanol; acetic acid / 10 h / 3102.89 Torr

With hydrogen; sodium acetate; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic anhydride; acetic acid; 1: Condensation / 2: Ring cleavage / 3: Catalytic hydrogenation;
DOI:10.1016/S0040-4020(00)00470-1