methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Base Information

Chemical Name:methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate
CAS No.:149982-07-0
Molecular Formula:C₃₁H₅₂O₄
Molecular Weight:488.751
Hs Code.:

Synonyms:methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Suppliers and Price of methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

There total 5 articles about methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 3-Methoxymethoxy-2-methyl-4-((E)-(7R,11R)-3,7,11,15-tetramethyl-hexadec-2-enyl)-benzoic acid

: 149982-07-0
methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Guidance literature:: In diethyl ether;
DOI:10.1002/hlca.19930760429

Reference yield:

: 7766-23-6
3-bromo-2-methylphenol

: 149982-07-0
methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / (i-Pr)2NEt / CH₂Cl₂; methyl acetate / 1 h / Ambient temperature

2: 1.) PhLi, 2.) CuBr / 1.) Et₂O, reflux, 7 h, 2.) EtO₂, r.t., overnight

3: 1.) tetramethylethylenediamine, BuLi / 1.) Et₂O, hexane, 0 deg C, 1 h, 2.) -25 deg C, 5 min

4: 57 percent / diethyl ether

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; phenyllithium; N-ethyl-N,N-diisopropylamine; copper(I) bromide; In diethyl ether; dichloromethane; acetic acid methyl ester;
DOI:10.1002/hlca.19930760429

Reference yield:

: 4444-13-7
phytyl bromide

: 149982-07-0
methyl 3-(methoxymethoxy)-2-methyl-phytylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) PhLi, 2.) CuBr / 1.) Et₂O, reflux, 7 h, 2.) EtO₂, r.t., overnight

2: 1.) tetramethylethylenediamine, BuLi / 1.) Et₂O, hexane, 0 deg C, 1 h, 2.) -25 deg C, 5 min

3: 57 percent / diethyl ether

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; phenyllithium; copper(I) bromide; In diethyl ether;
DOI:10.1002/hlca.19930760429