methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile
CAS No.:155205-41-7
Molecular Formula:C₂₉H₃₁NO₅
Molecular Weight:473.569
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

There total 10 articles about methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 773837-37-9
sodium cyanide

: 291753-79-2
methyl 2,3,4-tri-O-benzyl-6-deoxy-6-iodo-α-D-manno-pyranoside

: 155205-41-7
methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

Guidance literature:: In dimethyl sulfoxide; at 60 ℃; for 17h; Inert atmosphere;
DOI:10.1055/s-0035-1560572

Reference yield: 94.0%

: 10442-39-4
tetra-n-butylammonium cyanide

: 291753-79-2
methyl 2,3,4-tri-O-benzyl-6-deoxy-6-iodo-α-D-manno-pyranoside

: 155205-41-7
methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 25 ℃; for 3h;

Reference yield:

: 34212-64-1,641635-63-4
methyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 155205-41-7
methyl 2,3,4-tri-O-benzyl-6-deoxy-α-D-manno-heptopyranosylurononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / I₂; imidazole; PPh₃ / toluene / 1 h / 70 °C

2: 94 percent / dimethylformamide / 3 h / 0 - 25 °C

With 1H-imidazole; iodine; triphenylphosphine; In N,N-dimethyl-formamide; toluene;