N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide)

Base Information

Chemical Name:N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide)
CAS No.:211513-15-4
Molecular Formula:C₃₈H₅₆N₂O₂S₂
Molecular Weight:637.007
Hs Code.:

Synonyms:bis-[2-[1-(2-ethylbutyl)cyclohexanecarbonylamino]phenyl]disulfide

Suppliers and Price of N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide)

There total 4 articles about N,N'-(2,2'-disulfanediylbis(2,1-phenylene))bis(1-(2-ethylbutyl)cyclohexanecarboxaMide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 211515-46-7
1-(2-ethyl-butyl)-cyclohexanecarbonyl chloride

: 1141-88-4
2-Aminophenyl disulfide

: 211513-15-4
bis-[2-[1-(2-ethylbutyl)cyclohexanecarbonylamino]phenyl]disulfide

Guidance literature:: With pyridine; at 100 ℃;
DOI:10.1021/jm000224s

Reference yield:

: 381209-09-2
1-(2-ethyl-butyl)-cyclohexanecarboxylic acid

: 211513-15-4
bis-[2-[1-(2-ethylbutyl)cyclohexanecarbonylamino]phenyl]disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / oxalyl chloride / CH₂Cl₂ / 1 h / 20 °C

2: pyridine / 100 °C

With pyridine; oxalyl dichloride; In dichloromethane; 1: Chlorination / 2: Acylation;
DOI:10.1021/jm000224s

Reference yield:

: 3814-34-4
2-ethyl-1-bromobutane

: 211513-15-4
bis-[2-[1-(2-ethylbutyl)cyclohexanecarbonylamino]phenyl]disulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 1.5 h / 20 °C

1.2: tetrahydrofuran / 20 °C

2.1: 38 percent / oxalyl chloride / CH₂Cl₂ / 1 h / 20 °C

3.1: pyridine / 100 °C

With pyridine; oxalyl dichloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 1.1: Metallation / 1.2: Alkylation / 2.1: Chlorination / 3.1: Acylation;
DOI:10.1021/jm000224s