5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

Base Information

Chemical Name:5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide
CAS No.:1351237-97-2
Molecular Formula:C₂₅H₂₁N₅O₂S
Molecular Weight:455.54
Hs Code.:

Synonyms:5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

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Chemical Property of 5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

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Technology Process of 5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

There total 12 articles about 5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 896160-38-6
5-(3-(2-cyanopropan-2-yl)benzamido)-2-methylbenzoic acid

: 936361-27-2
thieno[2,3-b]pyrazin-6-amine

: 1351237-97-2
5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

Guidance literature:: 5-(3-(2-cyanopropan-2-yl)benzamido)-2-methylbenzoic acid; thieno[2,3-b]pyrazin-6-amine; With thionyl chloride; at 80 ℃; for 2h;

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: C₁₉H₁₇ClN₂O₂

: 936361-27-2
thieno[2,3-b]pyrazin-6-amine

: 1351237-97-2
5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 936361-26-1
tert-butyl thieno[2,3-b]pyrazin-6-ylcarbamate

: 1351237-97-2
5-(3-(2-cyanopropan-2-yl)benzamido)-2-methyl-N-(thieno[2,3-b]pyrazin-6-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;