Ethyl 2-methyl-5-nitrobenzoate

Base Information

Chemical Name:Ethyl 2-methyl-5-nitrobenzoate
CAS No.:124358-24-3
Molecular Formula:C10H11NO4
Molecular Weight:209.202
Hs Code.:2916399090
DSSTox Substance ID:DTXSID50594303
Wikidata:Q82489099
Mol file:124358-24-3.mol

Synonyms:Ethyl 2-methyl-5-nitrobenzoate;124358-24-3;2-METHYL-5-NITROBENZOIC ACID ETHYL ESTER;SCHEMBL550516;DTXSID50594303;Ethyl-2-Methyl-5-nitro benzoate;OWSPBONPFGBEFL-UHFFFAOYSA-N;MFCD11111004;AKOS009486127;DB-164483;F78616

Suppliers and Price of Ethyl 2-methyl-5-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
2-Methyl-5-nitrobenzoicacidethylester
5g
$ 1728.00

AHH
ethyl2-methyl-5-nitrobenzoate 97%
5g
$ 879.00

Total 4 raw suppliers

Chemical Property of Ethyl 2-methyl-5-nitrobenzoate

Chemical Property:

Vapor Pressure:0.000342mmHg at 25°C
Melting Point:30-31 °C
Boiling Point:319.3°C at 760 mmHg
Flash Point:142.1°C
PSA：72.12000
Density:1.216g/cm³
LogP:2.60310
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:209.06880783
Heavy Atom Count:15
Complexity:248

Purity/Quality:

99% ^*data from raw suppliers

2-Methyl-5-nitrobenzoicacidethylester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C1=C(C=CC(=C1)[N+](=O)[O-])C

Technology Process of Ethyl 2-methyl-5-nitrobenzoate

There total 1 articles about Ethyl 2-methyl-5-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 64-17-5
ethanol

: 1975-52-6
5-nitro-o-toluic acid

: 124358-24-3
ethyl 2-methyl-5-nitrobenzoate

Guidance literature:: With thionyl chloride; at 0 - 20 ℃; Heating / reflux;

Reference yield: 100.0%

: 124358-24-3
ethyl 2-methyl-5-nitrobenzoate

: 7335-32-2
ethyl 5-amino-2-methylbenzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;
DOI:10.1016/S0040-4039(98)00932-0

Reference yield:

: 124358-24-3
ethyl 2-methyl-5-nitrobenzoate

: 34265-55-9
ethyl 3-hydroxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethanol / Ambient temperature

2: 1.) NaNO₃, H₂SO₄, 2.) Cu(NO₃)2*2.5H₂O, Cu₂O / 1.) H₂O, 0 deg C, 2.) H₂O, rt

With copper(I) oxide; sodium nitrate; sulfuric acid; hydrogen; copper(II) nitrate; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4039(98)00932-0