[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Base Information

Chemical Name:[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene
CAS No.:177161-91-0
Molecular Formula:C₄₄H₅₆F₂₆O₃
Molecular Weight:1126.89
Hs Code.:

[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Synonyms:[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

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Chemical Property of [2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

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Technology Process of [2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

There total 4 articles about [2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 177161-59-0
12,12,13,13,14,14,15,15,15-nonafluoropentadecyl methanesulfonate

: 177161-90-9
3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

: 177161-91-0
[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; for 72h; Heating;
DOI:10.1002/hlca.19960790209

Reference yield:

: 1512-02-3
12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluorononadecanol

: 177161-91-0
[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / 5 h / -15 °C

2: 1.) NaH / 1.) THF, 4 h, room t. and 65 deg C, 45 min, 2.) THF, 3 days, reflux

3: 70 percent / 1.0M BH₃/THF / tetrahydrofuran / 60 h / 40 - 45 °C

4: 75 percent / 12N KOH, Bu₄N(HSO₄) / diethyl ether / 72 h / Heating

With tetrahydrofuran; pyridine; potassium hydroxide; borane; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1002/hlca.19960790209

Reference yield:

: 36096-97-6
12,12,13,13,14,14,15,15,15-nonafluoro-1-pentadecanol

: 177161-91-0
[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 5 h / -15 °C

2: 75 percent / 12N KOH, Bu₄N(HSO₄) / diethyl ether / 72 h / Heating

With pyridine; potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether;
DOI:10.1002/hlca.19960790209