3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

Base Information

Chemical Name:3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol
CAS No.:177161-90-9
Molecular Formula:C₂₉H₃₅F₁₇O₃
Molecular Weight:754.568
Hs Code.:

Synonyms:3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

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Chemical Property of 3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

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Technology Process of 3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

There total 2 articles about 3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 177161-89-6
5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane

: 177161-90-9
3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

Guidance literature:: With tetrahydrofuran; borane; In tetrahydrofuran; at 40 - 45 ℃; for 60h;
DOI:10.1002/hlca.19960790209

Reference yield:

: 1512-02-3
12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluorononadecanol

: 177161-90-9
3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 5 h / -15 °C

2: 1.) NaH / 1.) THF, 4 h, room t. and 65 deg C, 45 min, 2.) THF, 3 days, reflux

3: 70 percent / 1.0M BH₃/THF / tetrahydrofuran / 60 h / 40 - 45 °C

With tetrahydrofuran; pyridine; borane; sodium hydride; In tetrahydrofuran;
DOI:10.1002/hlca.19960790209

Reference yield: 75.0%

: 177161-59-0
12,12,13,13,14,14,15,15,15-nonafluoropentadecyl methanesulfonate

: 177161-90-9
3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

: 177161-91-0
[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In diethyl ether; for 72h; Heating;
DOI:10.1002/hlca.19960790209