8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate

Base Information

• Chemical Name: 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate
• CAS No.: 289697-75-2
• Molecular Formula: C₁₈H₁₇N₆O₉P
• Molecular Weight: 492.342

Synonyms:8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate

Chemical Property of 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate

Chemical Property:

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Technology Process of 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate

There total 2 articles about 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

4-Nitrophenacyl bromide (99-81-0) + 5'-adenosine monophosphate (61-19-8,24937-83-5,67583-85-1) → 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate (289697-75-2) + 8-(p-nitro-phenyl)-8-hydroxy-3-β-D-ribofuranosylimidazolino[2,1-i]purine-5'-mono-phosphate

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 20 ℃; for 12h; pH=4.5;

DOI:10.1080/15257770008033041

Reference yield:

8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-tri-phosphate (289697-76-3) → 8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate (289697-75-2)

Guidance literature:

With ATPDase from bovine spleen; In water; at 37 ℃; pH=7.6; Enzyme kinetics;

DOI:10.1080/15257770008033041

Reference yield:

8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate (289697-75-2) → 8-(p-amino-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate (748121-06-4)

Guidance literature:

With hydrogen; platinum(IV) oxide; In water; at 20 ℃; under 3154.6 Torr;

DOI:10.1080/15257770008033041

upstream raw materials:

4-Nitrophenacyl bromide

5'-adenosine monophosphate

8-(p-nitro-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-tri-phosphate

Downstream raw materials:

8-(p-amino-phenyl)-3-β-D-ribofuranosylimidazo[2,1-i]purine-5'-mono-phosphate

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