(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

Base Information

Chemical Name:(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O
CAS No.:1334715-07-9
Molecular Formula:C₅₂H₇₁GeOP
Molecular Weight:815.699
Hs Code.:

(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh<sub>2</sub>)O

Synonyms:(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

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Chemical Property of (2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

Chemical Property:

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Technology Process of (2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

There total 1 articles about (2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 438201-89-9
3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

: 525-06-4
diphenyl ketene

: 1334715-07-9
(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

Guidance literature:: In diethyl ether; at -80°C, to Et2O soln. of Ge compd., slowly added Et2O soln. of diphenylketene; monitored by NMR between -80°C and room temp.; isolated by cooling to -80°C;
DOI:10.1002/anie.201102500

Reference yield:

: 1334715-07-9
(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

: 525-06-4
diphenyl ketene

: (2,4,6-triisopropylphenyl)(tBu)GeC(CCPh₂)P(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

Guidance literature:: In diethyl ether; to Ge complex added Et2O soln. of diphenylketene; warmed to room temp.;
DOI:10.1002/anie.201102500

Reference yield:

: 1334715-07-9
(2,4,6-triisopropylphenyl)(tBu)GeCP(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

: (2,4,6-triisopropylphenyl)(tBu)GeCHCH₂C(CH₃)2P(2,4,6-tris-tert-butylphenyl)C(CPh₂)O

Guidance literature:: In diethyl ether; byproducts: LiF; Et2O soln. of Ge compd. slowly warmed to room temp.; solvent removed at reduced pressure, replaced with pentane; ppt. eliminated by filtration; concd., cooled to -20°C;
DOI:10.1002/anie.201102500