3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

Base Information

Chemical Name:3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene
CAS No.:438201-89-9
Molecular Formula:C₃₈H₆₁GeP
Molecular Weight:621.466
Hs Code.:

Synonyms:3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

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Chemical Property of 3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

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Technology Process of 3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

There total 6 articles about 3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 438201-93-5
(2,4,6-triisopropylphenyl)(t-Bu)Ge(F)C(Cl)P(2,4,6-tri-tert-butylphenyl)

: 438201-89-9
3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

Guidance literature:: With tert-butyllithium; In diethyl ether; pentane; byproducts: LiF, LiCl; to a soln. germallene in diethyl ether was added a soln. of tert-butyllithium in pentane cooled to -78°C; not isolated, detected by NMR spectra;
DOI:10.1021/ic1014913

Reference yield:

: 438201-91-3
tert-butyl-2,4,6-triisopropylphenyl(dimethoxy)germane

: 438201-89-9
3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

Guidance literature:: Multi-step reaction with 3 steps

1: water; benzene

2: t-BuLi / hexane; tetrahydrofuran

3: t-BuLi / pentane; diethyl ether

With t-BuLi; In tetrahydrofuran; diethyl ether; hexane; water; pentane; benzene;
DOI:10.1016/S0022-328X(01)01223-2

Reference yield:

: 438201-92-4
difluoro(2,4,6-triisopropylphenyl)(tert-butyl)germane

: 438201-89-9
3-(2,4,6-triisopropylphenyl)-3-tert-butyl-1-(2,4,6-tri-tert-butylphenyl)germaphosphaallene

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi / hexane; tetrahydrofuran

2: t-BuLi / pentane; diethyl ether

With t-BuLi; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1016/S0022-328X(01)01223-2