C₁₇⁽¹³⁾CH₂₀O₃Se

Base Information

Chemical Name:C₁₇⁽¹³⁾CH₂₀O₃Se
CAS No.:116757-31-4
Molecular Formula:C₁₈H₂₀O₃Se
Molecular Weight:364.304
Hs Code.:

C<sub>17</sub><sup>(13)</sup>CH<sub>20</sub>O<sub>3</sub>Se

Synonyms:C₁₇⁽¹³⁾CH₂₀O₃Se

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Chemical Property of C₁₇⁽¹³⁾CH₂₀O₃Se

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Technology Process of C₁₇⁽¹³⁾CH₂₀O₃Se

There total 5 articles about C₁₇⁽¹³⁾CH₂₀O₃Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₁₇⁽¹³⁾CH₂₀O₂Se

: 116757-31-4
C₁₇⁽¹³⁾CH₂₀O₃Se

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 0.25h;

Reference yield:

: 34598-65-7
α-phenylseleno propionic acid

: 116757-31-4
C₁₇⁽¹³⁾CH₂₀O₃Se

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / oxalyl chloride / 1,2-dichloro-ethane / 1.5 h / Ambient temperature

2: 84 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

3: 98 percent / 3 h / 160 - 180 °C

4: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.25 h / -78 °C

With oxalyl dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 1132-39-4
diphenylselenide

: 116757-31-4
C₁₇⁽¹³⁾CH₂₀O₃Se

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaBH₄ / 1.) EtOH, 0 deg C, 2.) EtOH, water, RT, overnight

2: 92 percent / oxalyl chloride / 1,2-dichloro-ethane / 1.5 h / Ambient temperature

3: 84 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

4: 98 percent / 3 h / 160 - 180 °C

5: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.25 h / -78 °C

With sodium tetrahydroborate; oxalyl dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1,2-dichloro-ethane;