6-fluoro-9,10-dihydrobenzopyrene

Base Information

• Chemical Name: 6-fluoro-9,10-dihydrobenzo
• Molecular Formula: C₂₀H₁₃F
• Molecular Weight: 272.322

Synonyms:6-fluoro-9,10-dihydrobenzopyrene

Chemical Property of 6-fluoro-9,10-dihydrobenzo

Chemical Property:

Purity/Quality:

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Useful:

There total 1 articles about 6-fluoro-9,10-dihydrobenzopyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

6-bromo-9,10-dihydrobenzopyrene (221347-73-5) → 9,10-dihydro benzopyrene (17573-15-8) + 6-fluoro-9,10-dihydrobenzopyrene (221347-74-6)

Guidance literature:

With tert.-butyl lithium; N-fluorobis(benzenesulfon)imide; In toluene; for 1.5h; Yields of byproduct given; Ambient temperature;

DOI:10.1021/jo9819178

Reference yield: 70.0%

6-fluoro-9,10-dihydrobenzopyrene (221347-74-6) → cis-7,8-dihydroxy-6-fluoro-7,8-dihydrobenzopyrene (83768-92-7)

Guidance literature:

With osmium(VIII) oxide; In pyridine; at 0 - 20 ℃; for 19h;

DOI:10.1021/jo9819178

Reference yield: 46.0%

silver benzoate (532-31-0) + 6-fluoro-9,10-dihydrobenzopyrene (221347-74-6) → trans-7,8-dibenzoyloxy-6-fluoro-7,8,9,10-tetrahydrobenzopyrene

Guidance literature:

With iodine; In benzene; Heating;

DOI:10.1021/jo9819178

upstream raw materials:

6-bromo-9,10-dihydrobenzopyrene

Downstream raw materials:

cis-7,8-dihydroxy-6-fluoro-7,8-dihydrobenzopyrene

(7R,8R)-6-fluoro-7,8-dihydroxy-7,8-dihydrobenzo[a]pyrene

(+/-)-trans-7,8-dihydroxy-6-fluoro-7,8-dihydrobenzopyrene

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