N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

Base Information

Chemical Name:N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide
CAS No.:1176196-98-7
Molecular Formula:C₁₃H₁₇IN₆O₅
Molecular Weight:464.22
Hs Code.:

Synonyms:N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

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Chemical Property of N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

Chemical Property:

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Technology Process of N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

There total 4 articles about N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.8%

: 1178872-46-2
methyl 2-(2-iodobenzamido)-5-(3-nitroguanidino)pentanoate

: 1176196-98-7
N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

Guidance literature:: With hydroxylamine potassium salt; In methanol; at 20 ℃;
DOI:10.1016/j.bmc.2009.04.056

Reference yield:

: 2149-70-4,13855-78-2,38733-00-5
N-nitro-L-arginine

: 1176196-98-7
N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride

2: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane

3: hydroxylamine potassium salt / methanol

With hydroxylamine potassium salt; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; acetyl chloride; In methanol; dichloromethane;
DOI:10.1007/s00044-017-1999-2

Reference yield:

: 74-79-3,25212-18-4
L-arginine

: 1176196-98-7
N-(1-(hydroxyamino)-5-(3-nitroguanidino)-1-oxopentan-2-yl)-2-iodobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; sulfuric acid

2: acetyl chloride

3: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane

4: hydroxylamine potassium salt / methanol

With hydroxylamine potassium salt; sulfuric acid; nitric acid; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; acetyl chloride; In methanol; dichloromethane;
DOI:10.1007/s00044-017-1999-2