N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

Base Information

Chemical Name:N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate
CAS No.:1448815-86-8
Molecular Formula:C₅H₁₁NO*C₁₈H₁₆N₄O₄S₂
Molecular Weight:517.63
Hs Code.:

Synonyms:N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

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Chemical Property of N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

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Technology Process of N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

There total 2 articles about N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 109-02-4
4-methyl-morpholine

: 39145-34-1
2-furfurylidenecyanothioacetamide

: 4542-32-9
N-[4-(aminosulfonyl)phenyl]-3-oxobutanamide

: 1448815-86-8
N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

Guidance literature:: In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/ml400226s

Reference yield:

: 63-74-1
sulfanilamide

: 1448815-86-8
N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / acetone / 1 h / Reflux; Inert atmosphere

2: ethanol / 20 °C / Inert atmosphere

With 4-methyl-morpholine; In ethanol; acetone;
DOI:10.1021/ml400226s

Reference yield: 84.0%

: 1448815-86-8
N-methylmorpholinium 5-({[4-(aminosulfonyl)phenyl]amino}carbonyl)-3-cyano-4-(2-furyl)-6-methyl-1,4-dihydropyridine-2-thiolate

: 20172-36-5
α-chloro-N-(p-ethylphenyl)acetamide

: 701245-18-3
N-[4-(aminosulfonyl)phenyl]-5-cyano-6-({2-[(4-ethylphenyl)amino]-2-oxoethyl}thio)-4-(2-furyl)-2-methyl-1,4-dihydropyridine-3-carboxamide

Guidance literature:: With potassium hydroxide; In ethanol; water; at 25 - 30 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ml400226s